TA Instruments

AR1721-0001f

04/09/2012 18:18:57

Sample name	ASW 10 mm from base, 60 mm to top, disk 22 Provil novo maximum texture REMOVED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1721
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 18:18:57

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-14.91	7.565	-1.971	1.0040	22.4	1909	5.3562	10000	0.4685	33.35	6.6952	669.52	3.383E-3	0.0	1.0	61.004	-45.745	6.052
0.7966	12.26	0.06495	2.0040	22.4	1919	13.1684	10000	0.4709	12.75	16.461	1646.1	3.384E-3	0.0	1.0	62.004	2.4441	9.812
1.538	19.33	0.07954	3.0000	22.4	1909	26.8103	10000	0.4685	5.106	33.513	3351.3	3.384E-3	0.1	1.1	63.000	4.7182	15.47
2.088	23.01	0.09074	4.0040	22.4	1910	40.8688	10000	0.4687	3.606	51.086	5108.6	3.384E-3	0.1	1.1	64.004	6.4060	18.41
3.314	30.83	0.1075	5.0040	22.4	1903	67.4887	10000	0.4671	2.002	84.361	8436.1	3.384E-3	0.1	1.1	65.004	10.166	24.66
5.036	39.47	0.1276	6.0040	22.4	1915	106.5900	10000	0.4699	1.229	133.24	13324	3.383E-3	0.1	1.1	66.004	15.451	31.58
5.808	42.52	0.1366	7.0120	22.4	1908	126.2270	10000	0.4683	1.055	157.78	15778	3.383E-3	0.1	1.1	67.012	17.817	34.02
7.348	49.12	0.1496	8.0080	22.4	1915	165.1720	10000	0.4701	0.7938	206.47	20647	3.383E-3	0.1	1.1	68.008	22.544	39.30
9.720	57.53	0.1690	9.0040	22.4	1911	223.0480	10000	0.4691	0.5775	278.81	27881	3.384E-3	0.2	1.2	69.004	29.820	46.02
11.72	63.68	0.1840	10.004	22.4	1895	274.6290	10000	0.4650	0.4672	343.29	34329	3.384E-3	0.2	1.2	70.004	35.948	50.94
13.77	69.64	0.1977	11.004	22.4	1910	325.9090	10000	0.4687	0.3937	407.39	40739	3.384E-3	0.2	1.2	71.004	42.240	55.71
15.63	75.11	0.2080	12.004	22.4	1896	377.0590	10000	0.4654	0.3361	471.32	47132	3.384E-3	0.2	1.2	72.004	47.939	60.09
17.29	80.50	0.2148	13.004	22.4	1899	434.7930	10000	0.4660	0.2930	543.49	54349	3.384E-3	0.2	1.2	73.004	53.056	64.40
19.43	86.43	0.2248	14.004	22.4	1903	498.5920	10000	0.4671	0.2548	623.24	62324	3.384E-3	0.2	1.2	74.004	59.608	69.14
22.72	94.60	0.2402	15.004	22.4	1894	594.0920	10000	0.4648	0.2116	742.62	74262	3.384E-3	0.3	1.3	75.004	69.717	75.68
24.61	99.90	0.2463	16.004	22.4	1892	664.1400	10000	0.4644	0.1896	830.18	83018	3.384E-3	0.3	1.3	76.004	75.506	79.92
27.01	105.7	0.2557	17.004	22.4	1896	740.6060	10000	0.4652	0.1698	925.76	92576	3.384E-3	0.3	1.3	77.004	82.874	84.53
30.37	113.7	0.2670	18.004	22.4	1898	854.9730	10000	0.4658	0.1467	1068.7	1.0687E5	3.383E-3	0.3	1.3	78.004	93.168	90.98
32.80	118.8	0.2761	19.004	22.4	1903	931.1930	10000	0.4671	0.1348	1164.0	1.1640E5	3.384E-3	0.3	1.3	79.004	100.63	95.04
35.04	124.2	0.2820	20.004	22.4	1886	1020.0900	10000	0.4630	0.1222	1275.1	1.2751E5	3.383E-3	0.3	1.3	80.004	107.49	99.40
38.87	132.3	0.2938	21.008	22.4	1875	1153.6899	10000	0.4602	0.1071	1442.1	1.4421E5	3.383E-3	0.4	1.4	81.008	119.25	105.8
41.19	137.4	0.2999	22.004	22.4	1889	1242.4600	10000	0.4636	0.1001	1553.1	1.5531E5	3.383E-3	0.4	1.4	82.004	126.38	109.9
43.48	142.8	0.3045	23.004	22.4	1885	1343.4600	10000	0.4626	0.09244	1679.3	1.6793E5	3.384E-3	0.4	1.4	83.004	133.41	114.2
47.74	150.8	0.3166	24.004	22.4	1875	1495.5100	10000	0.4602	0.08244	1869.4	1.8694E5	3.383E-3	0.4	1.4	84.004	146.47	120.6
49.79	155.9	0.3193	25.004	22.4	1872	1596.7700	10000	0.4593	0.07699	1996.0	1.9960E5	3.384E-3	0.4	1.4	85.004	152.76	124.7
53.01	161.3	0.3286	26.008	22.4	1870	1710.8000	10000	0.4589	0.07186	2138.5	2.1385E5	3.383E-3	0.4	1.4	86.008	162.64	129.1
57.84	169.3	0.3416	27.004	22.4	1867	1881.7600	10000	0.4583	0.06514	2352.2	2.3522E5	3.384E-3	0.5	1.5	87.004	177.45	135.4
60.77	174.4	0.3484	28.004	22.4	1858	1995.6700	10000	0.4561	0.06108	2494.6	2.4946E5	3.383E-3	0.5	1.5	88.004	186.43	139.5
63.27	179.5	0.3524	29.004	22.4	1856	2115.8701	10000	0.4555	0.05757	2644.8	2.6448E5	3.384E-3	0.5	1.5	89.004	194.10	143.6
68.34	187.5	0.3644	30.004	22.4	1859	2305.6699	10000	0.4563	0.05286	2882.1	2.8821E5	3.384E-3	0.5	1.5	90.004	209.65	150.0
70.71	192.7	0.3669	31.004	22.4	1843	2432.1201	10000	0.4524	0.04964	3040.2	3.0402E5	3.384E-3	0.5	1.5	91.004	216.93	154.2
73.51	197.8	0.3716	32.004	22.4	1842	2636.0300	10000	0.4520	0.04706	3295.0	3.2950E5	3.384E-3	0.5	1.5	92.004	225.54	158.3
78.88	205.8	0.3832	33.000	22.4	1849	2773.5701	10000	0.4539	0.04365	3467.0	3.4670E5	3.384E-3	0.6	1.6	93.000	241.99	164.7
82.32	211.0	0.3902	34.004	22.4	1843	2913.2600	10000	0.4524	0.04142	3641.6	3.6416E5	3.383E-3	0.6	1.6	94.004	252.57	168.8
87.01	218.6	0.3980	35.004	22.4	1828	3128.8401	10000	0.4486	0.03825	3911.1	3.9111E5	3.384E-3	0.6	1.6	95.004	266.93	174.9
91.20	223.9	0.4073	36.004	22.4	1827	3282.3899	10000	0.4484	0.03644	4103.0	4.1030E5	3.383E-3	0.6	1.6	96.004	279.80	179.1
94.27	229.1	0.4115	37.004	22.4	1827	3431.7800	10000	0.4484	0.03481	4289.7	4.2897E5	3.383E-3	0.6	1.6	97.004	289.23	183.3
99.47	236.6	0.4204	38.004	22.4	1809	3657.8601	10000	0.4439	0.03230	4572.3	4.5723E5	3.384E-3	0.6	1.6	98.004	305.18	189.3
102.6	241.8	0.4242	39.004	22.4	1812	3822.0801	10000	0.4447	0.03099	4777.6	4.7776E5	3.384E-3	0.7	1.7	99.004	314.75	193.5
106.9	249.6	0.4282	40.004	22.4	1805	4068.4700	10000	0.4431	0.02898	5085.6	5.0856E5	3.383E-3	0.7	1.7	100.004	327.88	199.7
109.8	254.6	0.4314	41.004	22.4	1826	4237.4102	10000	0.4482	0.02817	5296.8	5.2968E5	3.383E-3	0.7	1.7	101.004	337.01	203.7
113.9	259.8	0.4384	42.004	22.4	1819	4409.3398	10000	0.4466	0.02695	5511.7	5.5117E5	3.384E-3	0.7	1.7	102.004	349.44	207.9
118.6	267.6	0.4430	43.004	22.4	1815	4674.4302	10000	0.4453	0.02534	5843.0	5.8430E5	3.384E-3	0.7	1.7	103.004	363.74	214.1
123.0	272.7	0.4510	44.004	22.4	1800	4851.1299	10000	0.4417	0.02421	6063.9	6.0639E5	3.383E-3	0.7	1.7	104.004	377.25	218.1
129.9	280.3	0.4634	45.004	22.4	1781	5129.7202	10000	0.4370	0.02266	6412.2	6.4122E5	3.384E-3	0.8	1.8	105.004	398.58	224.3
133.3	285.5	0.4668	46.004	22.4	1797	5320.2598	10000	0.4411	0.02205	6650.3	6.6503E5	3.384E-3	0.8	1.8	106.004	408.89	228.4
139.6	293.1	0.4762	47.004	22.4	1772	5601.9199	10000	0.4348	0.02062	7002.4	7.0024E5	3.383E-3	0.8	1.8	107.004	428.26	234.5
142.5	298.1	0.4781	48.004	22.4	1774	5797.4199	10000	0.4354	0.01996	7246.8	7.2468E5	3.383E-3	0.8	1.8	108.004	437.33	238.5
146.7	303.3	0.4835	49.004	22.4	1765	5999.3599	10000	0.4332	0.01918	7499.2	7.4992E5	3.384E-3	0.8	1.8	109.004	449.96	242.7
151.1	311.0	0.4859	50.004	22.4	1783	6302.0898	10000	0.4376	0.01844	7877.6	7.8776E5	3.384E-3	0.8	1.8	110.004	463.59	248.8
157.4	316.0	0.4982	51.004	22.4	1780	6515.0400	10000	0.4368	0.01782	8143.8	8.1438E5	3.384E-3	0.9	1.9	111.004	483.02	252.8
163.9	323.8	0.5063	52.008	22.4	1764	6831.8398	10000	0.4330	0.01683	8539.8	8.5398E5	3.384E-3	0.9	1.9	112.008	502.94	259.0
167.7	328.9	0.5098	53.004	22.4	1762	7046.5000	10000	0.4326	0.01630	8808.1	8.8081E5	3.384E-3	0.9	1.9	113.004	514.40	263.1
173.4	336.4	0.5155	54.004	22.4	1754	7374.3901	10000	0.4305	0.01550	9218.0	9.2180E5	3.384E-3	0.9	1.9	114.004	532.07	269.1
176.7	341.6	0.5174	55.004	22.4	1761	7601.2402	10000	0.4322	0.01509	9501.6	9.5016E5	3.383E-3	0.9	1.9	115.004	542.22	273.3
181.2	346.7	0.5226	56.008	22.4	1729	7828.2900	10000	0.4242	0.01438	9785.4	9.7854E5	3.383E-3	0.9	1.9	116.008	555.90	277.4
188.1	354.2	0.5310	57.004	22.4	1721	8168.6499	10000	0.4224	0.01372	10211	1.0211E6	3.383E-3	1.0	2.0	117.004	577.00	283.4
193.3	359.4	0.5380	58.000	22.4	1729	8409.5703	10000	0.4244	0.01339	10512	1.0512E6	3.384E-3	1.0	2.0	118.000	593.13	287.5
198.2	367.0	0.5400	59.004	22.4	1720	8767.5098	10000	0.4222	0.01277	10959	1.0959E6	3.384E-3	1.0	2.0	119.004	607.96	293.6
203.2	372.0	0.5464	60.004	22.4	1695	9007.4102	10000	0.4159	0.01225	11259	1.1259E6	3.383E-3	1.0	2.0	120.004	623.55	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

207.3	375.0	0.5527	0.99600	22.4	1703	302.2270	10000	0.4180	0.01211	377.78	37778	3.384E-3	0.0	2.0	121.996	635.93	300.0
205.7	375.0	0.5486	1.9960	22.4	1748	550.6920	10000	0.4289	0.01243	688.37	68837	3.384E-3	0.0	2.0	122.996	631.14	300.0
206.0	375.0	0.5494	2.9960	22.4	1697	927.6080	10000	0.4165	0.01207	1159.5	1.1595E5	3.384E-3	0.0	2.1	123.996	632.11	300.0
205.2	375.0	0.5472	3.9960	22.4	1712	1179.1300	10000	0.4202	0.01217	1473.9	1.4739E5	3.384E-3	0.1	2.1	124.996	629.60	300.0
205.9	375.0	0.5491	4.9960	22.4	1738	1430.4301	10000	0.4267	0.01236	1788.0	1.7880E5	3.384E-3	0.1	2.1	125.996	631.71	300.0
205.1	375.0	0.5470	5.9960	22.4	1719	1809.2300	10000	0.4218	0.01222	2261.5	2.2615E5	3.384E-3	0.1	2.1	126.996	629.36	300.0
210.7	375.0	0.5620	7.0000	22.4	1685	2058.7900	10000	0.4135	0.01198	2573.5	2.5735E5	3.383E-3	0.1	2.1	128.000	646.56	300.0
205.6	375.0	0.5483	7.9960	22.4	1691	2437.6599	10000	0.4149	0.01202	3047.1	3.0471E5	3.383E-3	0.1	2.1	128.996	630.87	300.0
206.3	375.0	0.5503	9.1520	22.4	1715	2687.0000	10000	0.4210	0.01220	3358.8	3.3588E5	3.383E-3	0.2	2.2	130.152	633.06	300.0
207.2	375.0	0.5525	10.056	22.4	1732	2938.5200	10000	0.4251	0.01232	3673.2	3.6732E5	3.384E-3	0.2	2.2	131.056	635.61	300.0
208.0	375.0	0.5546	11.004	22.4	1752	3316.8101	10000	0.4299	0.01246	4146.0	4.1460E5	3.384E-3	0.2	2.2	132.004	638.10	300.0
203.4	375.0	0.5424	12.000	22.4	1742	3567.5500	10000	0.4275	0.01239	4459.4	4.4594E5	3.384E-3	0.2	2.2	133.000	624.07	300.0
206.9	375.0	0.5517	12.996	22.4	1710	3818.0100	10000	0.4196	0.01216	4772.5	4.7725E5	3.383E-3	0.2	2.2	133.996	634.73	300.0
205.1	375.0	0.5468	14.052	22.4	1724	4196.1602	10000	0.4232	0.01226	5245.2	5.2452E5	3.384E-3	0.2	2.3	135.052	629.10	300.0
204.2	375.0	0.5446	15.000	22.4	1727	4446.2402	10000	0.4238	0.01228	5557.8	5.5578E5	3.384E-3	0.3	2.3	136.000	626.54	300.0
203.8	375.0	0.5435	16.004	22.4	1746	4823.4702	10000	0.4285	0.01242	6029.3	6.0293E5	3.384E-3	0.3	2.3	137.004	625.30	300.0
204.8	375.0	0.5461	17.004	22.4	1735	5074.6299	10000	0.4259	0.01234	6343.3	6.3433E5	3.384E-3	0.3	2.3	138.004	628.29	300.0
210.0	375.0	0.5599	17.992	22.4	1705	5327.0698	10000	0.4184	0.01212	6658.8	6.6588E5	3.384E-3	0.3	2.3	138.992	644.19	300.0
206.7	375.0	0.5512	18.996	22.4	1745	5704.9302	10000	0.4283	0.01241	7131.2	7.1312E5	3.384E-3	0.3	2.3	139.996	634.15	300.0
208.6	375.0	0.5564	19.996	22.4	1723	5955.5098	10000	0.4228	0.01225	7444.4	7.4444E5	3.383E-3	0.3	2.3	140.996	640.06	300.0
208.5	375.0	0.5560	20.996	22.4	1708	6336.0498	10000	0.4192	0.01215	7920.1	7.9201E5	3.383E-3	0.3	2.4	141.996	639.69	300.0
209.3	375.0	0.5583	21.996	22.4	1714	6582.5200	10000	0.4206	0.01219	8228.2	8.2282E5	3.383E-3	0.4	2.4	142.996	642.25	300.0
205.0	375.0	0.5467	22.996	22.4	1731	6833.8901	10000	0.4249	0.01231	8542.4	8.5424E5	3.384E-3	0.4	2.4	143.996	628.98	300.0
209.8	375.0	0.5594	24.000	22.4	1712	7223.2002	10000	0.4202	0.01217	9029.0	9.0290E5	3.383E-3	0.4	2.4	145.000	643.54	300.0
207.1	375.0	0.5523	24.996	22.4	1732	7462.2300	10000	0.4251	0.01231	9327.8	9.3278E5	3.383E-3	0.4	2.4	145.996	635.37	300.0
208.4	375.0	0.5558	25.996	22.4	1705	7713.6699	10000	0.4184	0.01212	9642.1	9.6421E5	3.384E-3	0.4	2.4	146.996	639.45	300.0
205.2	375.0	0.5472	26.996	22.4	1719	8090.6499	10000	0.4218	0.01222	10113	1.0113E6	3.384E-3	0.4	2.5	147.996	629.56	300.0
204.4	375.0	0.5452	27.996	22.4	1719	8341.9697	10000	0.4218	0.01222	10427	1.0427E6	3.383E-3	0.5	2.5	148.996	627.18	300.0
208.3	375.0	0.5555	29.004	22.4	1723	8718.8301	10000	0.4228	0.01225	10899	1.0899E6	3.384E-3	0.5	2.5	150.004	639.12	300.0
206.9	375.0	0.5518	29.996	22.4	1732	8970.1797	10000	0.4251	0.01232	11213	1.1213E6	3.383E-3	0.5	2.5	150.996	634.88	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

205.4	370.5	0.5544	1.0240	22.4	1701	292.8950	10000	0.4175	0.01239	366.12	36612	3.383E-3	0.0	2.5	152.024	630.17	296.4
198.8	365.5	0.5439	2.0160	22.4	1724	533.4490	10000	0.4232	0.01291	666.81	66681	3.384E-3	0.0	2.6	153.016	609.93	292.4
190.4	357.9	0.5321	3.0120	22.4	1733	887.7760	10000	0.4253	0.01353	1109.7	1.1097E5	3.383E-3	0.1	2.6	154.012	584.23	286.3
188.7	352.7	0.5351	4.0160	22.4	1713	1125.8000	10000	0.4204	0.01377	1407.3	1.4073E5	3.383E-3	0.1	2.6	155.016	579.05	282.2
178.0	347.7	0.5121	5.0200	22.4	1761	1465.5200	10000	0.4322	0.01457	1831.9	1.8319E5	3.383E-3	0.1	2.6	156.020	546.25	278.1
176.9	340.1	0.5202	5.9960	22.4	1748	1689.2600	10000	0.4289	0.01511	2111.6	2.1116E5	3.383E-3	0.1	2.6	156.996	542.75	272.0
174.7	334.9	0.5217	7.0160	22.4	1754	1916.8900	10000	0.4305	0.01564	2396.1	2.3961E5	3.383E-3	0.1	2.6	158.016	536.04	267.9
165.6	327.4	0.5057	8.0160	22.4	1768	2234.0100	10000	0.4340	0.01650	2792.5	2.7925E5	3.384E-3	0.1	2.7	159.016	507.94	261.9
165.6	322.3	0.5137	9.0200	22.4	1765	2446.9800	10000	0.4332	0.01699	3058.7	3.0587E5	3.384E-3	0.2	2.7	160.020	507.90	257.8
158.5	314.5	0.5038	10.016	22.4	1769	2767.1299	10000	0.4342	0.01788	3458.9	3.4589E5	3.384E-3	0.2	2.7	161.016	486.13	251.6
152.4	309.5	0.4925	11.016	22.4	1784	2967.2300	10000	0.4378	0.01862	3709.0	3.7090E5	3.384E-3	0.2	2.7	162.016	467.61	247.6
147.8	304.4	0.4854	12.000	22.4	1774	3168.6699	10000	0.4354	0.01914	3960.8	3.9608E5	3.383E-3	0.2	2.7	163.000	453.36	243.6
142.4	296.7	0.4798	13.016	22.4	1797	3467.0400	10000	0.4411	0.02041	4333.8	4.3338E5	3.383E-3	0.2	2.7	164.016	436.74	237.4
139.9	291.5	0.4798	14.000	22.4	1793	3660.9299	10000	0.4401	0.02110	4576.2	4.5762E5	3.384E-3	0.2	2.8	165.000	429.13	233.2
131.7	284.0	0.4638	15.000	22.4	1790	3942.9299	10000	0.4393	0.02220	4928.7	4.9287E5	3.384E-3	0.3	2.8	166.000	404.01	227.2
129.2	278.8	0.4635	16.016	22.4	1801	4130.3198	10000	0.4421	0.02317	5162.9	5.1629E5	3.384E-3	0.3	2.8	167.016	396.44	223.0
124.5	271.1	0.4592	17.020	22.4	1786	4399.1699	10000	0.4384	0.02430	5499.0	5.4990E5	3.384E-3	0.3	2.8	168.020	381.96	216.9
119.6	266.1	0.4495	18.016	22.4	1810	4574.3999	10000	0.4441	0.02555	5718.0	5.7180E5	3.384E-3	0.3	2.8	169.016	366.97	212.9
115.5	261.0	0.4426	19.016	22.4	1808	4749.7300	10000	0.4437	0.02655	5937.2	5.9372E5	3.384E-3	0.3	2.8	170.016	354.33	208.8
110.3	253.2	0.4359	20.016	22.4	1804	5005.9800	10000	0.4427	0.02815	6257.5	6.2575E5	3.384E-3	0.3	2.9	171.016	338.54	202.5
107.1	248.1	0.4314	21.000	22.4	1820	5174.5601	10000	0.4468	0.02956	6468.2	6.4682E5	3.384E-3	0.4	2.9	172.000	328.43	198.5
102.0	240.4	0.4241	22.016	22.4	1815	5414.8501	10000	0.4453	0.03140	6768.6	6.7686E5	3.384E-3	0.4	2.9	173.016	312.82	192.3
97.02	235.1	0.4126	23.000	22.4	1830	5576.1001	10000	0.4492	0.03311	6970.1	6.9701E5	3.383E-3	0.4	2.9	174.000	297.64	188.1
93.60	230.0	0.4069	24.000	22.4	1836	5724.9399	10000	0.4506	0.03470	7156.2	7.1562E5	3.383E-3	0.4	2.9	175.000	287.16	184.0
90.15	222.3	0.4055	25.020	22.4	1823	5950.0000	10000	0.4474	0.03688	7437.5	7.4375E5	3.383E-3	0.4	2.9	176.020	276.58	177.9
86.56	217.0	0.3988	26.020	22.4	1847	6102.3799	10000	0.4533	0.03920	7628.0	7.6280E5	3.384E-3	0.4	3.0	177.020	265.55	173.6
80.19	209.5	0.3828	27.004	22.4	1846	6306.1001	10000	0.4531	0.04207	7882.6	7.8826E5	3.384E-3	0.5	3.0	178.004	246.01	167.6
78.46	204.3	0.3840	28.016	22.4	1848	6443.4800	10000	0.4535	0.04426	8054.4	8.0544E5	3.383E-3	0.5	3.0	179.016	240.70	163.5
75.44	199.1	0.3790	29.016	22.4	1841	6582.5498	10000	0.4518	0.04646	8228.2	8.2282E5	3.384E-3	0.5	3.0	180.016	231.43	159.2
69.63	191.3	0.3641	30.016	22.4	1872	6774.4702	10000	0.4593	0.05117	8468.1	8.4681E5	3.383E-3	0.5	3.0	181.016	213.63	153.0
66.33	186.1	0.3563	31.020	22.4	1865	6899.3101	10000	0.4577	0.05383	8624.1	8.6241E5	3.383E-3	0.5	3.0	182.020	203.49	148.9
63.50	178.2	0.3564	32.020	22.4	1859	7087.8901	10000	0.4563	0.05856	8859.9	8.8599E5	3.384E-3	0.5	3.1	183.020	194.82	142.5
59.02	173.1	0.3410	33.016	22.4	1862	7198.8101	10000	0.4571	0.06216	8998.5	8.9985E5	3.384E-3	0.6	3.1	184.016	181.08	138.5
57.62	168.0	0.3430	34.016	22.4	1859	7311.1699	10000	0.4563	0.06587	9139.0	9.1390E5	3.383E-3	0.6	3.1	185.016	176.78	134.4
52.49	160.1	0.3279	35.016	22.4	1870	7479.9502	10000	0.4589	0.07299	9349.9	9.3499E5	3.384E-3	0.6	3.1	186.016	161.03	128.0
49.46	154.7	0.3197	36.000	22.4	1873	7585.3999	10000	0.4598	0.07827	9481.8	9.4818E5	3.384E-3	0.6	3.1	187.000	151.73	123.8
48.13	149.6	0.3217	37.016	22.4	1879	7685.1299	10000	0.4612	0.08393	9606.4	9.6064E5	3.384E-3	0.6	3.1	188.016	147.65	119.7
43.06	141.7	0.3039	38.016	22.4	1884	7834.5898	10000	0.4624	0.09384	9793.2	9.7932E5	3.384E-3	0.6	3.2	189.016	132.10	113.4
40.62	136.1	0.2983	39.016	22.4	1879	7934.5898	10000	0.4612	0.1014	9918.2	9.9182E5	3.384E-3	0.7	3.2	190.016	124.61	108.9
38.19	130.9	0.2917	40.016	22.4	1880	8021.3398	10000	0.4614	0.1097	10027	1.0027E6	3.384E-3	0.7	3.2	191.016	117.16	104.7
34.37	122.9	0.2796	41.016	22.4	1884	8152.0200	10000	0.4624	0.1246	10190	1.0190E6	3.384E-3	0.7	3.2	192.016	105.45	98.36
32.19	117.3	0.2743	42.016	22.4	1884	8238.9404	10000	0.4624	0.1368	10299	1.0299E6	3.383E-3	0.7	3.2	193.016	98.746	93.88
29.66	112.1	0.2646	43.020	22.4	1880	8313.5303	10000	0.4614	0.1496	10392	1.0392E6	3.383E-3	0.7	3.2	194.020	90.995	89.69
26.34	104.1	0.2530	44.016	22.4	1891	8425.2803	10000	0.4640	0.1744	10532	1.0532E6	3.384E-3	0.7	3.3	195.016	80.812	83.29
24.01	98.42	0.2440	45.020	22.4	1899	8499.7100	10000	0.4660	0.1960	10625	1.0625E6	3.384E-3	0.8	3.3	196.020	73.664	78.74
21.56	93.17	0.2314	46.000	22.4	1910	8561.7402	10000	0.4687	0.2200	10702	1.0702E6	3.384E-3	0.8	3.3	197.000	66.133	74.53
19.56	87.86	0.2226	47.016	22.4	1895	8623.7002	10000	0.4650	0.2454	10780	1.0780E6	3.384E-3	0.8	3.3	198.016	59.999	70.29
17.35	82.23	0.2110	48.020	22.4	1905	8717.2998	10000	0.4677	0.2818	10897	1.0897E6	3.384E-3	0.8	3.3	199.020	53.224	65.79
14.86	73.96	0.2010	49.016	22.4	1906	8765.8604	10000	0.4679	0.3484	10957	1.0957E6	3.383E-3	0.8	3.3	200.016	45.602	59.17
13.29	68.60	0.1937	50.016	22.4	1903	8815.4102	10000	0.4671	0.4043	11019	1.1019E6	3.384E-3	0.8	3.4	201.016	40.770	54.88
11.26	62.80	0.1793	51.020	22.4	1921	8864.3799	10000	0.4715	0.4871	11080	1.1080E6	3.383E-3	0.9	3.4	202.020	34.539	50.24
9.555	56.85	0.1681	52.016	22.4	1901	8907.3301	10000	0.4666	0.5882	11134	1.1134E6	3.384E-3	0.9	3.4	203.016	29.315	45.48
7.427	48.75	0.1523	53.016	22.4	1917	8963.3896	10000	0.4705	0.8066	11204	1.1204E6	3.384E-3	0.9	3.4	204.016	22.784	39.00
5.884	42.53	0.1384	54.016	22.4	1923	8999.1201	10000	0.4719	1.063	11249	1.1249E6	3.384E-3	0.9	3.4	205.016	18.053	34.02
4.514	35.98	0.1254	55.000	22.4	1909	9029.4697	10000	0.4685	1.474	11287	1.1287E6	3.384E-3	0.9	3.4	206.000	13.848	28.79
3.394	30.32	0.1119	56.016	22.4	1908	9053.6904	10000	0.4683	2.075	11317	1.1317E6	3.384E-3	0.9	3.5	207.016	10.412	24.26
2.867	27.09	0.1059	57.108	22.4	1910	9077.0596	10000	0.4689	2.604	11346	1.1346E6	3.384E-3	1.0	3.5	208.108	8.7965	21.67
1.619	19.27	0.08399	58.020	22.4	1925	9088.4297	10000	0.4725	5.184	11361	1.1361E6	3.384E-3	1.0	3.5	209.020	4.9658	15.42
0.7822	12.37	0.06322	59.044	22.4	1929	9099.5898	10000	0.4735	12.60	11374	1.1374E6	3.384E-3	1.0	3.5	210.044	2.3999	9.899
0.4640	8.339	0.05564	60.016	22.4	1927	9104.5195	10000	0.4729	27.71	11381	1.1381E6	3.384E-3	1.0	3.5	211.016	1.4234	6.671

